Assay Method Information

Assay Name:  Homogeneous time resolved fluorescence (HTRF)
Description:  The identified compounds were tested for their capacity to inhibit the PD-1/PD-L1 interaction using in vitro functional assays. Homogeneous time resolved fluorescence (HTRF) was used to evaluate those 94 hits identified in silico. The BMS202 inhibitor, known as a small-molecule inhibitor of PD-1/PD-L1 interaction, was used as a reference. Compounds were tested at 100 μM and the determination of the inhibition levels was based on the HTRF signal reduction. Hits were defined as compounds that inhibited at least 50% of the PD-1/PD-L1 interaction.
Affinity data for this assay
 

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