Assay Method Information

Assay Name:  ATR Biochemical Assay
Description:  ATR enzyme (batch: Eurofins Cat. No. 14-953) solutions were prepared in 1x kinase base buffer. 10 ul of 2x enzyme solution (final concentration: 2.5 nM) was added to each well of the 384-well assay plate containing 60 nl compound in each well. The plate was incubated at room temperature for 10 minutes. 2x peptide solutions were prepared with FAM-labeled peptide and ATP in the 1x kinase base buffer. 10 ul of 2x peptide solution was added to each well of the 384-well assay plate, which was incubated at 28 C. for 240 min. 40 ul of stop buffer was added to stop reaction. Data were collected by Caliper.
Affinity data for this assay
 

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